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Endocrine Assay Validation: T4, Cortisol, Progesterone, Relaxin

1. Scope

Endocrine testing is a cornerstone of veterinary internal medicine, but hormone assays are analytically demanding: analytes are present at low concentrations, are often unstable pre-analytically, and reference ranges are species- and context-dependent. This document summarizes the validation of Migibio's four core endocrine assays.

Assay Primary Use Species
T4 (Total Thyroxine) Hypo/hyperthyroidism screening Canine, Feline
TSH Hypothyroidism confirmation Canine
Cortisol Cushing's / Addison's (adrenal) Canine
Progesterone Breeding / ovulation timing Canine
Relaxin Pregnancy confirmation Canine, Feline

2. Clinical Rationale

2.1 Thyroid — T4 & TSH

  • T4 is the primary screening test for thyroid function in dogs and cats.
  • TSH is measured in combination with T4 to differentiate primary hypothyroidism (high TSH + low T4) from euthyroid sick syndrome.
  • Feline hyperthyroidism is diagnosed by elevated T4; ~10% of early cases have normal T4 but elevated free T4.

2.2 Cortisol — Adrenal Function

  • Basal cortisol alone is insufficient; dynamic testing (ACTH stimulation / low-dose dexamethasone suppression) is standard.
  • FICT provides rapid quantitative cortisol to support same-visit adrenal evaluation.

2.3 Progesterone — Breeding Management

  • Progesterone is the gold standard for ovulation timing — the single highest-value endocrine test in breeding practice.
  • Serial measurement (every 2–3 days) pinpoints the LH surge and optimal mating/AI window.

2.4 Relaxin — Pregnancy

  • Relaxin is produced by the placenta; detection confirms pregnancy from ~day 21–28 in dogs and cats.
  • Differentiates pregnancy from pseudopregnancy.

3. Reference Ranges

Analyte Species Reference Range Unit
T4 (Total) Canine 1.0–4.0 µg/dL
T4 (Total) Feline 1.0–4.0 µg/dL
TSH Canine 0–0.6 ng/mL
Cortisol (basal) Canine 2–6 µg/dL
Progesterone (anestrus) Canine 0–2 ng/mL
Relaxin (pregnant) Canine/Feline > 1.0 ng/mL

4. Analytical Performance

Analyte LOD Linear Range Intra-assay CV% Inter-assay CV%
T4 0.1 µg/dL 0.2–10 µg/dL < 8% < 10%
TSH 0.03 ng/mL 0.05–5 ng/mL < 8% < 10%
Cortisol 0.2 µg/dL 0.5–30 µg/dL < 8% < 10%
Progesterone 0.2 ng/mL 0.5–40 ng/mL < 8% < 10%
Relaxin 0.1 ng/mL 0.3–20 ng/mL < 8% < 10%

5. Interpretation Notes

  • T4 low + TSH high → primary hypothyroidism (canine).
  • Progesterone > 2 ng/mL then rapid rise to > 5 ng/mL → ovulation window (breed/AI within 24–48 h).
  • Relaxin > 1 ng/mL at day 21–28 → pregnancy confirmed.
  • Cortisol should always be interpreted with clinical signs and, where indicated, dynamic testing.

For structured per-analyte data, see the Data Hub. For methodology, see Validation Methodology.

Authored by: Migibio Clinical & Scientific Affairs, Guangzhou Magic Biotech Co., Ltd.

Reviewed by: Migibio R&D Quality Committee

Last updated: 2026-08-13

Disclosure: Migibio (Guangzhou Magic Biotech Co., Ltd.) is the manufacturer of the FIA680/FIA880 analyzers and FICT reagents referenced in this content. See our Editorial & Review Policy.

Contact: Martin.Wong  ·  Phone (WhatsApp): +86 13323237275  ·  Email: [email protected]
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